N-(2-溴苄氧羰氧基)丁二酰胺

Name	Carbonicacidbromobenzylsuccinimidylester
Synonyms	2-BrZ-OSU Z(2-Br)OSu 2-BR-Z-OSU Z(2-Br)-OSu 2-BR-Z-ONSU Z-(2-Br)-Osu LABOTEST-BB LT00453236 N-(2-BROMO-Z) SUCCINIMIDE 2-Bromobenzyl succinimdyl carbonate 2-BROMOBENZYL SUCCINIMDYL CARBONATE 2-BROMOBENZYL SUCCINIMIDYL CARBONATE 2-Bromobenzyl Succinimidyl Carbonate 2-BROMOBENZYL-N-SUCCINIMIDYL CARBONATE Carbonicacidbromobenzylsuccinimidylester N-(2-Bromobenzyloxycarbonyloxy)succinimide N-(2-Bromobenzyloxy Carbonyloxy)Succinimide CARBONIC ACID 2-BROMOBENZYL SUCCINIMIDYL ESTER Carbonic acid 2-Bromobenzyl succinimidyl ester 1-({[(2-bromobenzyl)oxy]carbonyl}oxy)pyrrolidine-2,5-dione
CAS	128611-93-8
InChI	InChI=1/C12H10BrNO5/c13-9-4-2-1-3-8(9)7-18-12(17)19-14-10(15)5-6-11(14)16/h1-4H,5-7H2
InChIKey	SZDNRTVADOCWKU-UHFFFAOYSA-N

Molecular Formula	C12H10BrNO5
Molar Mass	328.12
Density	1.70±0.1 g/cm3(Predicted)
Melting Point	105-108°C
Boling Point	418.2±47.0 °C(Predicted)
Flash Point	206.7°C
Vapor Presure	3.35E-07mmHg at 25°C
Appearance	White solid
BRN	3623239
Storage Condition	Inert atmosphere,2-8°C
Sensitive	Moisture Sensitive
Refractive Index	1.621
MDL	MFCD00082848
Use	Used as amino acid Protectant

Hazard Symbols	Xn - Harmful
Risk Codes	43 - May cause sensitization by skin contact
Safety Description	S22 - Do not breathe dust. S36/37 - Wear suitable protective clothing and gloves. S24/25 - Avoid contact with skin and eyes. S36 - Wear suitable protective clothing. S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S37 - Wear suitable gloves. S24 - Avoid contact with skin.
UN IDs	3335
HS Code	29339990
Hazard Class	9

application	2-bromobenzyl-N-succinimide carbonate is an organic intermediate, which can be prepared from 2-bromobenzyl alcohol and N,N'-disuccinimide carbonate in one step, and can be used in laboratory research and development process and chemical production process.
preparation	n is added to the solution of 2-bromobenzyl alcohol (2.83g,15.0 mmol,1.0 equivalent) and DMAP(916 mg,7.5 mmol,0.5 equivalent) in MeCN/DCM 1:1(45 mL), n'-disuccinimide carbonate (3.84g,15.0 mmol,1.0 equivalents). The mixture was continuously stirred at room temperature for 18 hours. The mixture was washed with H2O(1 × 45mL), saturated NaHCO3, sodium chloride solution (1 × 45mL), dried with MgSO4, filtered and concentrated in vacuum. The residue was recrystallized from iPrOH to give 2-bromobenzyl-N-succinimidyl carbonate.
use	as amino acid protective agent

Last Update：2024-04-09 21:54:55

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