N,N-DIBENZYL-FORMAMIDE - Names and Identifiers
Name | N,N-dibenzylformamide
|
Synonyms | NSC 5982 Dibenzylformamide N,N-dibenzylformamide N,N-Dibenzylformamide N,N-DIBENZYL-FORMAMIDE N,N-bis(benzyl)formamide Formamide, N,N-dibenzyl- N,N-bis(phenylmethyl)formamide N,N-bis(phenylmethyl)methanamide formamide, N,N-bis(phenylmethyl)- Formamide, N,N-bis(phenylmethyl)-
|
CAS | 5464-77-7
|
InChI | InChI=1/C15H15NO/c17-13-16(11-14-7-3-1-4-8-14)12-15-9-5-2-6-10-15/h1-10,13H,11-12H2 |
N,N-DIBENZYL-FORMAMIDE - Physico-chemical Properties
Molecular Formula | C15H15NO
|
Molar Mass | 225.29 |
Density | 1.104±0.06 g/cm3(Predicted) |
Melting Point | 51-53°C |
Boling Point | 217 °C(Press: 12 Torr) |
Flash Point | 159.4°C |
Solubility | Chloroform |
Vapor Presure | 1.79E-07mmHg at 25°C |
Appearance | Solid |
Color | White |
pKa | -0.50±0.70(Predicted) |
Storage Condition | Sealed in dry,Room Temperature |
Refractive Index | 1.5782 (589.3 nm 25℃ |
N,N-DIBENZYL-FORMAMIDE - Introduction
N,N-dibenzylformamide(N,N-dibenzylformamide) is an organic compound with the chemical formula C16H15NO. It is a colorless liquid with a strong pungent odor of azone at room temperature. The following is an introduction to the nature, use, preparation and safety information of N,N-dibenzylformamide:
Nature:
-Appearance: N, the N-dibenzylformamide is a colorless liquid, but it can usually be slightly yellow.
-Solubility: It can be dissolved in many organic solvents, such as alcohols, ethers and aromatic hydrocarbons.
-Melting point: N, the melting point of N-dibenzylformamide is 20-23°C.
-Boiling point: Its boiling point is 200-210°C.
-Density: N, the density of the N-dibenzylformamide is about 1.06g/cm³.
Use:
- N,N-dibenzylformamide is commonly used as a solvent in organic synthesis. It can be used as an intermediate in the reaction between amine compounds and amides, and can also be used as a solvent in the hydrogenation reagent.
-It can also be used in industrial applications such as the preparation of dyes, dye intermediates and preservatives.
Preparation Method:
- N,N-dibenzylformamide can be prepared by the reaction of benzyl magnesium bromide and formyl chloride. First, benzyl magnesium bromide is reacted with formyl chloride to produce benzyl acyl formate, which is then hydrolyzed to produce N,N-dibenzylformamide.
-In addition, it can also be obtained by reacting formic anhydride and benzylamine under base catalysis.
Safety Information:
- N,N-dibenzylformamide irritant to skin and eyes, avoid contact with skin and eyes.
-When using this compound, pay attention to good ventilation conditions and avoid using fire sources.
-Should be stored in a cool, dry place, away from fire and oxidizing agents.
-Wear personal protective equipment such as protective gloves, goggles, and protective clothing when using or handling N,N-dibenzylformamide. If exposed to the compound by accident, rinse immediately with plenty of water and seek medical help.
Last Update:2024-04-10 22:29:15