104934-52-3
3-DODECYLTHIOPHENE
CAS: 104934-52-3
Molecular Formula: C16H28S
104934-52-3 - Names and Identifiers
| Name | 3-DODECYLTHIOPHENE |
| Synonyms | K0290 S1033 3-Laurylthiophene 3-DODECYLTHIOPHENE 3-N-LAURYLTHIOPHENE 3-N-DODECYLTHIOPHENE Thiophene,3-dodecyl- 1-(Thien-3-yl)dodecane 3-(Dodec-1-yl)thiophene |
| CAS | 104934-52-3 |
| InChI | InChI=1/C16H28S/c1-2-3-4-5-6-7-8-9-10-11-12-16-13-14-17-15-16/h13-15H,2-12H2,1H3 |
| InChIKey | RFKWIEFTBMACPZ-UHFFFAOYSA-N |
104934-52-3 - Physico-chemical Properties
| Molecular Formula | C16H28S |
| Molar Mass | 252.46 |
| Density | 0.902 g/mL at 25 °C (lit.) |
| Melting Point | -0.15°C (estimate) |
| Boling Point | 290 °C (lit.) |
| Flash Point | >230°F |
| Vapor Presure | 0.000276mmHg at 25°C |
| Appearance | clear liquid |
| Color | Colorless to Light yellow |
| Storage Condition | 2-8°C |
| Refractive Index | n20/D 1.488(lit.) |
| Physical and Chemical Properties | Storage Conditions: 0-6 ℃ WGK Germany:3 |
104934-52-3 - Risk and Safety
| Safety Description | 24/25 - Avoid contact with skin and eyes. |
| WGK Germany | 3 |
| HS Code | 29339900 |
104934-52-3 - Reference Information
| Overview | under N2 atmosphere, to contain magnesium dust (3.28g,0.135mol), anhydrous THF(30ml) A solution of 1-bromododecane (28.75g,26.9mL,0.13mol) in anhydrous THF(45mL) was added slowly to a mL three-necked flask with a small amount of iodine mixture. After the mixture was refluxed at 70 ° C. For 2 hours, the system was cooled to room temperature with ice water, and Ni(dppp)Cl2(0.54g, 1.00mmol) was added first, A solution of 3-bromothiophene (16.31g,0.10mol) in dry THF(40ml) was added slowly. The mixed solution was stirred overnight at room temperature and the reaction was quenched by the addition of cold aqueous HCl(1.50mol/L). The crude product was extracted with dichloromethane, dried over anhydrous magnesium sulfate, and further purified by chromatography column separation purification (n-hexane as eluent) to give a clear liquid (22.18g,88%). 1H NMR(300MHz,CDCl3): Δ7.22 (m,1H),6.95(m,2H),2.63(t,2H), 1.65(m,2H),1.32(m,18h),0.89(t,3H). |
| Application | 3-dodecylthiophene is an organic intermediate, it can be prepared from 3-bromothiophene and halogenated hydrocarbon in one step and can be used to prepare photoelectric materials. |
| Use | conductive polymer precursor |
Last Update：2024-04-09 21:04:16
Supplier List
Spot supply
Product Name: Thiophene3-dodecyl- Visit Supplier Webpage Request for quotationCAS: 104934-52-3
Tel: +86 0571-86722205
Email: sales@chinaskyrun.com
Mobile: +8618958170122
QQ: 2531159185
Wechat: chinaskyrun
Spot supply
Product Name: 3-Dodecylthiophene Visit Supplier Webpage Request for quotationCAS: 104934-52-3
Tel: +86-400-900-4166
Email: product@acmec-e.com
Mobile: +86-18621343501
QQ: 2881950922
Wechat: 18621343501
WhatsApp: +86-18621343501
Spot supply
Product Name: 3-Dodecylthiophene Visit Supplier Webpage Request for quotationCAS: 104934-52-3
Tel: +86-18821248368
Email: Int06@meryer.com
Mobile: +86-18821248368
QQ: 495145328
WhatsApp: +86-18821248368
Spot supply
Product Name: Thiophene3-dodecyl- Visit Supplier Webpage Request for quotationCAS: 104934-52-3
Tel: +86 0571-86722205
Email: sales@chinaskyrun.com
Mobile: +8618958170122
QQ: 2531159185
Wechat: chinaskyrun
Spot supply
Product Name: 3-Dodecylthiophene Visit Supplier Webpage Request for quotationCAS: 104934-52-3
Tel: +86-400-900-4166
Email: product@acmec-e.com
Mobile: +86-18621343501
QQ: 2881950922
Wechat: 18621343501
WhatsApp: +86-18621343501
Spot supply
Product Name: 3-Dodecylthiophene Visit Supplier Webpage Request for quotationCAS: 104934-52-3
Tel: +86-18821248368
Email: Int06@meryer.com
Mobile: +86-18821248368
QQ: 495145328
WhatsApp: +86-18821248368
View History
104934-52-3
RARECHEM AK HC S197
68178-51-8
telluriumfluoride(tef6)
四芬-D12
heptafluoro-butanenitril
AKOS PAO-1141
613656-90-9
1-[3-(3,4-dimethoxyphenyl)acryloyl]-2,2,4-trimethyl-4-phenyl-1,2,3,4-tetrahydroquinoline
21937-59-7
RARECHEM AK HC S197
68178-51-8
telluriumfluoride(tef6)
四芬-D12
heptafluoro-butanenitril
AKOS PAO-1141
613656-90-9
1-[3-(3,4-dimethoxyphenyl)acryloyl]-2,2,4-trimethyl-4-phenyl-1,2,3,4-tetrahydroquinoline
21937-59-7