双(2-氯乙基)胺盐酸盐
Bis(2-chloroethyl)amine hydrochloride
CAS: 821-48-7
Molecular Formula: C4H9Cl2N·HCl
双(2-氯乙基)胺盐酸盐 - Names and Identifiers
双(2-氯乙基)胺盐酸盐 - Physico-chemical Properties
| Molecular Formula | C4H9Cl2N·HCl |
| Molar Mass | 178.49 |
| Melting Point | 212-214℃ |
| Boling Point | 204.2°C at 760 mmHg |
| Flash Point | 77.3°C |
| Water Solubility | SOLUBLE |
| Vapor Presure | 0.267mmHg at 25°C |
| Appearance | Morphological Crystalline Powder |
| Color | White to beige |
| BRN | 3550356 |
| Storage Condition | Store below +30°C. |
| Sensitive | Hygroscopic |
| MDL | MFCD00012515 |
| Use | Used as a pharmaceutical Intermediate |
双(2-氯乙基)胺盐酸盐 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | R36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. |
| UN IDs | 2811 |
| WGK Germany | 3 |
| RTECS | IA1225000 |
| TSCA | Yes |
| HS Code | 29211980 |
| Hazard Class | 8 |
| Packing Group | III |
| Toxicity | LD50 orally in Rabbit: 1150 mg/kg |
双(2-氯乙基)胺盐酸盐 - Upstream Downstream Industry
双(2-氯乙基)胺盐酸盐 - Nature
| Solubility | >100g/l |
| NIST chemical information | 2,2'-Dichlorodiethylamine hydrochloride(821-48-7) |
| EPA chemical information | Ethanamine, 2-chloro-N-(2-chloroethyl)-, hydrochloride (821-48-7) |
Last Update：2024-04-10 22:29:15
双(2-氯乙基)胺盐酸盐 - Security information
| Hazard Note | Irritant/Toxic |
Last Update：2024-04-10 22:29:15
双(2-氯乙基)胺盐酸盐 - Uses and synthesis methods
Production method
It is obtained by the reaction of diethanolamine and thionyl chloride. Dissolve thionyl chloride in chloroform, and drop a mixture of diethanolamine and chloroform below 0°C. Control the droplet acceleration to maintain the temperature at -4-6 ℃. After adding, keep the temperature and stir for 30min. Stir at room temperature for 1h, heat to 60-65 ℃, after all crystallization is precipitated, add anhydrous ethanol, heat and reflux to dissolve all. Pour out while hot, cool naturally, and precipitate crystals. Filter the next day and wash twice with chloroform or absolute ethanol. Dry to obtain a finished product with a 76% yield.
category
Toxic substances
Toxicity classification
Highly toxic
Acute toxicity
abdominal cavity-rat LD50: 100 mg/kg; Subcutaneous-mouse LD50: 20 mg/kg
flammability hazard characteristics
Combustible; combustion produces toxic nitrogen oxides, chloride and hydrogen chloride smoke
storage and transportation features
The warehouse is ventilated and dry at low temperature; stored separately from food ingredients
Fire extinguishing agent
Dry powder, foam, sand, carbon dioxide, mist water
Last Update：2024-04-09 20:52:54
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View History
双(2-氯乙基)胺盐酸盐
1-BENZYL-4-PIPERIDONE HCL
Oxybisbenzoic acid
甲硝唑苯甲酸酯
5-氯噻吩-2-亚磺酸钠
苄基三苯基膦氯化物
硅烷,四氢化硅
乙氧亚氨基乙酸乙酯
全氟甲基乙烯基醚(PMVE)
胺-PEG3-生物素(TFA)
1-BENZYL-4-PIPERIDONE HCL
Oxybisbenzoic acid
甲硝唑苯甲酸酯
5-氯噻吩-2-亚磺酸钠
苄基三苯基膦氯化物
硅烷,四氢化硅
乙氧亚氨基乙酸乙酯
全氟甲基乙烯基醚(PMVE)
胺-PEG3-生物素(TFA)
Raw Materials for 双(2-氯乙基)胺盐酸盐
Downstream Products for 双(2-氯乙基)胺盐酸盐
1-CYCLOPROPYLPIPERAZINE
N-(3-Trifluoromethylphenyl)piperazine
4-CYANO-4-PHENYLPIPERIDINE HYDROCHLORIDE
1-(3-FLUOROPHENYL)PIPERAZINE
1-(1-PHENYLETHYL)PIPERAZINE
1-(3-Chlorophenyl)piperazine dihydrochloride
1-(3,4-Dichlorophenyl)piperazine
1-[2-(MORPHOLIN-4-YL)-ETHYL]-PIPERAZINE
1-(3-METHYLPHENYL)PIPERAZINE
1-(2-ETHOXYPHENYL)PIPERAZINE HYDROCHLORIDE
1-(4-Chlorophenyl)piperazine
1-(2-Methylphenyl)piperazine
1-(1-NAPHTHYL)PIPERAZINE HYDROCHLORIDE
N-(3-Trifluoromethylphenyl)piperazine
4-CYANO-4-PHENYLPIPERIDINE HYDROCHLORIDE
1-(3-FLUOROPHENYL)PIPERAZINE
1-(1-PHENYLETHYL)PIPERAZINE
1-(3-Chlorophenyl)piperazine dihydrochloride
1-(3,4-Dichlorophenyl)piperazine
1-[2-(MORPHOLIN-4-YL)-ETHYL]-PIPERAZINE
1-(3-METHYLPHENYL)PIPERAZINE
1-(2-ETHOXYPHENYL)PIPERAZINE HYDROCHLORIDE
1-(4-Chlorophenyl)piperazine
1-(2-Methylphenyl)piperazine
1-(1-NAPHTHYL)PIPERAZINE HYDROCHLORIDE