TRZ11
2,4,6-TRIS(4-AMINOPHENYL)-1,3,5-TRIAZINE
CAS: 14544-47-9
Molecular Formula: C21H18N6
TRZ11 - Names and Identifiers
TRZ11 - Physico-chemical Properties
| Molecular Formula | C21H18N6 |
| Molar Mass | 354.408 |
| Density | 1.303±0.06 g/cm3(Predicted) |
| Melting Point | 380-382℃ |
| Boling Point | 705.2±70.0 °C(Predicted) |
| pKa | 3.68±0.10(Predicted) |
| Storage Condition | Keep in dark place,Sealed in dry,Room Temperature |
| Use | Uses 2,4, 6-tris (4-aminophenyl)-1,3, 5-triazine is a heterocyclic organic compound, which is used as a pharmaceutical raw material. |
TRZ11 - Risk and Safety
| UN IDs | 2811 |
| Hazard Class | 6.1 |
| Packing Group | Ⅲ |
TRZ11 - Preparation
preparation method of 2,4,6-tris (4-aminophenyl)-1,3, 5-triazine: 1.18g(10mmol) of p-aminobenzonitrile is added to a 50mL four-mouth flask, 25mL dichloromethane is added under magnetic stirring to dissolve it, 4mL(45mmol) trifluoromethanesulfonic acid is slowly added dropwise in an ice bath, and N2 protection reaction is completed for 24 hours. After the reaction is over, the lower yellow oil layer is separated, 20mL of water is added, and then the pH is adjusted to 9-11 with 50% sodium hydroxide solution, light yellow solid is precipitated, and the product 2,4, 6-tris (4-aminophenyl)-1,3, 5-triazine 993mg is obtained by suction filtration, washing and drying, with a yield of 85.0%.
Last Update：2024-04-09 21:11:58
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View History
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