MN(TMHD)3
Tris(2,2,6,6-tetramethyl-3,5-heptanedionato)manganese(III)
CAS: 14324-99-3
Molecular Formula: C33H57MnO6
MN(TMHD)3 - Names and Identifiers
MN(TMHD)3 - Physico-chemical Properties
| Molecular Formula | C33H57MnO6 |
| Molar Mass | 604.74 |
| Melting Point | 165°C |
| Boling Point | 255°C |
| Appearance | crystal |
| Color | black |
| Storage Condition | under inert gas (nitrogen or Argon) at 2-8°C |
| Sensitive | 4: no reaction with water under neutral conditions |
MN(TMHD)3 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S36/37 - Wear suitable protective clothing and gloves. |
| WGK Germany | 3 |
MN(TMHD)3 - Reference Information
| Introduction | Tris (2,2,6, 6-tetramethyl-3, 5-heptenoic acid) manganese is an intermetallic organic compound and can be prepared by reacting manganese (II) sulfate monohydrate with 2,2,6, 6-tetramethyl-3, 5-heptanedione. |
| preparation | at room temperature, to manganese (II) sulfate monohydrate (1.5g, 9 mmol, 1.0 eq) and 2,2,6, 6-tetramethyl-3, 5-heptanedione (5.0g, 27 mmol, 4.0 eq) in water (30 mL) A concentrated ammonia solution (12 mL) was added dropwise to the mixture with methanol (6 mL), resulting in the immediate formation of a dark olive green/brown precipitate. The precipitate was filtered off, washed with water (3x 10ml) and dried under vacuum for 24 hours to give Mn(dpm)3(4.9g,90%). The X-ray quality crystal of the complex was obtained from isopropanol. The results showed that the structure was tris (2,2,6, 6-tetramethyl-3, 5-heptenoic acid) Manganese, yield (4.9g,90%). |
Last Update：2024-04-10 22:29:15
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