17024-12-3
9-IODOPHENANTHRENE
CAS: 17024-12-3
Molecular Formula: C14H9I
17024-12-3 - Names and Identifiers
| Name | 9-IODOPHENANTHRENE |
| Synonyms | 9-IODOPHENANTHRENE 9-Phenanthryl iodide Phenanthrene, 9-iodo- 2,5-bis(4-ethoxyanilino)-3,6-dimethoxycyclohexa-2,5-diene-1,4-dione |
| CAS | 17024-12-3 |
| InChIKey | CBFIPOTVFMLMFQ-UHFFFAOYSA-N |
17024-12-3 - Physico-chemical Properties
| Molecular Formula | C14H9I |
| Molar Mass | 304.13 |
| Density | 1.692±0.06 g/cm3(Predicted) |
| Melting Point | 91-93 °C (lit.) |
| Boling Point | 411.0±14.0 °C(Predicted) |
| Storage Condition | Keep in dark place,Sealed in dry,Room Temperature |
| Stability | Stable, but light sensitive - store in the dark. Incompatible with strong oxidizing agents. |
17024-12-3 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. |
| WGK Germany | 3 |
17024-12-3 - Introduction
9-IODOPHENANTHRENE(9-IODOPHENANTHRENE) is an organic compound containing an iodine atom with the chemical formula C14H9I. It is a yellow solid, soluble in organic solvents such as ethanol and dichloromethane.
9-IODOPHENANTHRENE has important applications in organic synthesis. Due to its strong electron attracting property, it can be used as a reagent in allylation reaction, electrophilic substitution reaction and other organic reactions. In addition, 9-IODOPHENANTHRENE has applications in biomedical research as a fluorescent marker or probe.
A common method for preparing 9-IODOPHENANTHRENE is by reacting iodobenzene and benzo [α] fluorene (phenanthrene) under alkaline conditions. First, iodobenzene and benzo [α] fluorene are dissolved in an alkaline solvent such as acetonitrile or methylene chloride. Then, a basic catalyst such as sodium powder or potassium powder is added. The reaction is generally carried out at a temperature of 80-100 ° C. And the 9-IODOPHENANTHRENE product can be obtained.
When using 9-IODOPHENANTHRENE, you need to pay attention to its safety. It is a toxic substance that may irritate the skin, eyes and respiratory system. Therefore, appropriate protective equipment such as chemical gloves, goggles and protective masks should be worn during operation. At the same time, make sure to operate in a well-ventilated laboratory environment to avoid inhaling harmful gases. If contact or inhalation occurs, wash immediately or seek medical attention.
9-IODOPHENANTHRENE has important applications in organic synthesis. Due to its strong electron attracting property, it can be used as a reagent in allylation reaction, electrophilic substitution reaction and other organic reactions. In addition, 9-IODOPHENANTHRENE has applications in biomedical research as a fluorescent marker or probe.
A common method for preparing 9-IODOPHENANTHRENE is by reacting iodobenzene and benzo [α] fluorene (phenanthrene) under alkaline conditions. First, iodobenzene and benzo [α] fluorene are dissolved in an alkaline solvent such as acetonitrile or methylene chloride. Then, a basic catalyst such as sodium powder or potassium powder is added. The reaction is generally carried out at a temperature of 80-100 ° C. And the 9-IODOPHENANTHRENE product can be obtained.
When using 9-IODOPHENANTHRENE, you need to pay attention to its safety. It is a toxic substance that may irritate the skin, eyes and respiratory system. Therefore, appropriate protective equipment such as chemical gloves, goggles and protective masks should be worn during operation. At the same time, make sure to operate in a well-ventilated laboratory environment to avoid inhaling harmful gases. If contact or inhalation occurs, wash immediately or seek medical attention.
Last Update：2024-04-10 22:29:15
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