15522-59-5
tetrabutylammonium tetraphenylborate
CAS: 15522-59-5
Molecular Formula: C40H56BN
15522-59-5 - Names and Identifiers
| Name | tetrabutylammonium tetraphenylborate |
| Synonyms | TETRAPHENYLBORON TETRABUTYLAMMONIUM tetrabutylammonium tetraphenylborate TETRABUTYLAMMONIUM TETRAPHENYLBORATE Tetra-n-butylammonium tetraphenylborate TETRA-N-BUTYLAMMONIUM TETRAPHENYLBORATE ammonium,tetrabutyl-,tetraphenylborate(1-) N,N,N-Tributyl-1-Butanaminium tetraphenylborate(1-) N,N,N-tributylbutan-1-aminium tetraphenylborate(1-) |
| CAS | 15522-59-5 |
| EINECS | 239-562-9 |
| InChI | InChI=1/C24H20B.C16H36N/c1-5-13-21(14-6-1)25(22-15-7-2-8-16-22,23-17-9-3-10-18-23)24-19-11-4-12-20-24;1-5-9-13-17(14-10-6-2,15-11-7-3)16-12-8-4/h1-20H;5-16H2,1-4H3/q-1;+1 |
15522-59-5 - Physico-chemical Properties
| Molecular Formula | C40H56BN |
| Molar Mass | 561.69 |
| Melting Point | 230-236°C(lit.) |
| Water Solubility | Soluble in pyridine, acetone, water. |
| Solubility | acetonitrile: 0.1g/mL, clear, colorless |
| Appearance | powder to crystal |
| Color | White to Almost white |
| BRN | 3857215 |
| Storage Condition | Keep in dark place,Inert atmosphere,Room temperature |
| Stability | Stable. Incompatible with strong oxidizing agents. Hygroscopic. |
| Sensitive | Hygroscopic |
| MDL | MFCD00011749 |
15522-59-5 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. |
| WGK Germany | 3 |
| FLUKA BRAND F CODES | 8-9 |
15522-59-5 - Introduction
Tetrabuutylammonium tetraphenylborate is an Organoboron compound. The following is a description of its nature, use, preparation and safety information:
Nature:
- tetrabutylammonium tetraphenylborate is a colorless to pale yellow crystal.
-It has low solubility in water, but good solubility in organic solvents.
-It has good thermal and chemical stability.
Use:
- tetrabutylammonium tetraphenylborate is commonly used as a catalyst and ligand in organic synthesis.
-It can be used to catalyze chemical reactions, such as coupling reactions and addition reactions.
-It can also be used in the synthesis of organometallic compounds, organic photoelectric materials and organic batteries.
Method:
The preparation of tetrabutylammonium tetraphenylborate is usually carried out by the following steps:
1. The reaction of Phenylboronic acid and tetra-n-butyl ammonium bromide generates tetra-n-butyl tetraphenylboronic acid ammonium bromide.
2. React tetra-n-butyl tetraphenylborate ammonium bromide with sodium hydroxide to generate tetrabutylammonium tetraphenylborate.
Safety Information:
- tetrabutylammonium tetraphenylborate has low toxicity, but safety measures for correct operation should still be followed.
-When using, avoid inhaling its dust or solution, and avoid contact with skin and eyes.
-Wear appropriate protective gloves and glasses when handling.
-Maintain good ventilation during storage and handling.
-If accidental contact occurs, rinse immediately with plenty of water and seek medical help.
Nature:
- tetrabutylammonium tetraphenylborate is a colorless to pale yellow crystal.
-It has low solubility in water, but good solubility in organic solvents.
-It has good thermal and chemical stability.
Use:
- tetrabutylammonium tetraphenylborate is commonly used as a catalyst and ligand in organic synthesis.
-It can be used to catalyze chemical reactions, such as coupling reactions and addition reactions.
-It can also be used in the synthesis of organometallic compounds, organic photoelectric materials and organic batteries.
Method:
The preparation of tetrabutylammonium tetraphenylborate is usually carried out by the following steps:
1. The reaction of Phenylboronic acid and tetra-n-butyl ammonium bromide generates tetra-n-butyl tetraphenylboronic acid ammonium bromide.
2. React tetra-n-butyl tetraphenylborate ammonium bromide with sodium hydroxide to generate tetrabutylammonium tetraphenylborate.
Safety Information:
- tetrabutylammonium tetraphenylborate has low toxicity, but safety measures for correct operation should still be followed.
-When using, avoid inhaling its dust or solution, and avoid contact with skin and eyes.
-Wear appropriate protective gloves and glasses when handling.
-Maintain good ventilation during storage and handling.
-If accidental contact occurs, rinse immediately with plenty of water and seek medical help.
Last Update：2024-04-09 15:17:53
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