108612-54-0
4-N-Boc-4-N-Methyl-aminopiperidine
CAS: 108612-54-0
Molecular Formula: C11H22N2O2
108612-54-0 - Names and Identifiers
108612-54-0 - Physico-chemical Properties
| Molecular Formula | C11H22N2O2 |
| Molar Mass | 214.3 |
| Density | 1.01±0.1 g/cm3(Predicted) |
| Melting Point | 50°C(lit.) |
| Boling Point | 287.9±29.0 °C(Predicted) |
| Flash Point | 127.9°C |
| Vapor Presure | 0.00242mmHg at 25°C |
| Appearance | lens powder |
| pKa | 10.05±0.10(Predicted) |
| Storage Condition | under inert gas (nitrogen or Argon) at 2–8 °C |
| Refractive Index | 1.485 |
| MDL | MFCD02683051 |
108612-54-0 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S28 - After contact with skin, wash immediately with plenty of soap-suds. S36 - Wear suitable protective clothing. S44 - |
| HS Code | 29339900 |
| Hazard Note | Irritant |
108612-54-0 - Reference Information
| application | 4-N-tert-butoxycarbonyl-4-N-methylaminopiperidine can be used as an intermediate in organic synthesis and pharmaceutical intermediates, mainly used in laboratory research and development process and chemical production process. |
| Preparation | Pd(OH)2(14.11mg,0.1mmol) is added to a solution of 1-(benzyloxycarbonyl)-4-(N-methyl-tert-butoxycarbonylamino) piperidine (0.35g,1mmol) in anhydrous MeOH(20mL), the resulting mixture was stirred at room temperature for 2 hours in an H2 atmosphere. After TLC shows that the starting material is consumed, the solvent is filtered through silica gel and the filtrate solvent is removed in vacuum to obtain crude 4-(N-methyl-tert-butoxycarbonylamino) piperidine (0.2g,60%). |
Last Update：2024-04-09 21:01:54
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View History
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