104224-68-2
2-(1-Adamantyl)-4-bromophenol
CAS: 104224-68-2
Molecular Formula: C16H19BrO
104224-68-2 - Names and Identifiers
| Name | 2-(1-Adamantyl)-4-bromophenol |
| Synonyms | 2-(1-Adamantyl)-4-br 4-BROMO-2-ADAMANTYL PHENOL (2-ADAMANTYL)-4-BROMOPHENOL 2-ADAMANTANE-4-BROMOANISOLE 2-(1-Adamantyl)-4-bromophenol 2-(2-adamantyl)-4-bromophenol 2-(1-ADAMANTYL)-4-BROMOPHENOL 2-(Adamantan-1-yl)-4-bromophenol 2-(1-Adamantyl)-4-bromophenol (Adapalene) 4-bromo-2-tricyclo[3.3.1.1~3,7~]dec-1-ylphenol |
| CAS | 104224-68-2 |
| InChI | InChI=1/C16H19BrO/c17-13-1-2-15(18)14(6-13)16-7-10-3-11(8-16)5-12(4-10)9-16/h1-2,6,10-12,18H,3-5,7-9H2/t10-,11-,12-,16- |
104224-68-2 - Physico-chemical Properties
| Molecular Formula | C16H19BrO |
| Molar Mass | 307.23 |
| Density | 1.442±0.06 g/cm3(Predicted) |
| Melting Point | 137-141 |
| Boling Point | 392.0±35.0 °C(Predicted) |
| Flash Point | 190.9°C |
| Vapor Presure | 1.04E-06mmHg at 25°C |
| pKa | 9.56±0.43(Predicted) |
| Storage Condition | Inert atmosphere,Room Temperature |
| Refractive Index | 1.633 |
104224-68-2 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Hazard Note | Irritant |
104224-68-2 - Reference Information
| Application | 2-(1-adamantyl)-4-bromophenol can be used as an intermediate in pharmaceutical synthesis, can be prepared from 4-bromophenol as the reaction raw material, and can be used to prepare 3-(1-adamantyl)-4-benzyloxy bromide. |
| preparation | method 1: 4-bromophenol (0.346g,0.002mol) and 1-adamantanol (0.152g,0.001mol) and 1-bromoadamantane (0.022g,0.0001mol)(reagent molar ratio 2:1:0.1) are mixed in an ampoule and heated at 60 ℃ for C2 hours, the reaction mixture was cooled and treated with NaOH solution (2%) to remove excess 4-bromophenol, and the 2-(1-adamantyl)-4-bromophenol product was recrystallized from isooctane with a yield of 0.255g(83%) at mp148-149 °C. |
Last Update：2024-04-09 21:04:16
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View History
104224-68-2
AKOS B030092
SODIUM 2-ETHYLHEXYL SULFATE
一硝基苯
149696-13-9
126727-02-4
氨基乙酰氯
177853-64-4
沙夫卡因
1822672-88-7
AKOS B030092
SODIUM 2-ETHYLHEXYL SULFATE
一硝基苯
149696-13-9
126727-02-4
氨基乙酰氯
177853-64-4
沙夫卡因
1822672-88-7