1028206-60-1
RuPhos Pd G1 Methyl t--Butyl Ether Adduct
CAS: 1028206-60-1
Molecular Formula: C43H65ClNO3PPd
1028206-60-1 - Names and Identifiers
1028206-60-1 - Physico-chemical Properties
| Molecular Formula | C43H65ClNO3PPd |
| Molar Mass | 816.827861 |
| Appearance | Form Powder, color off-white to beige |
| Storage Condition | Inert atmosphere,2-8°C |
1028206-60-1 - Introduction
Chloro (2-dicyclohexylphosphino-2 ',6'-di1-propoxy-1, 1 '-biphenyl)[2-(2-aminoethylphenyl)] palladium (II), methyl tert-butyl ether (RuPhos Pd G1 Methyl t-Butyl Ether Adduct) is a palladium complex containing a phenyl group and a phosphorus-based ligand. It has the following characteristics:
Nature:
-Appearance: Colorless to light yellow crystal
-Molecular formula: Cover? H? ClNOP? Pd
-Molecular weight: 714.57g/mol
-Melting point: 160-161°C
-Soluble: Soluble in some organic solvents, such as dimethylformamide and dichloromethane
Use:
- RuPhos Pd G1 Methyl t-Butyl Ether Adduct is a commonly used palladium ligand system, which is widely used in organic synthesis reactions, especially negative hydrogenation reactions, hydrogenation coupling reactions and carbonylation reactions.
-The ligand has excellent catalytic activity and selectivity, can catalyze the hydrogenation reaction of a variety of substrates, and help improve the yield of the reaction and the purity of the product.
Preparation Method:
RuPhos Pd G1 Methyl t-Butyl Ether Adduct can be prepared by the following steps:
1. reacting dicyclohexylphosphino-2 ',6'-di I-propoxy -1,1 '-biphenyl with 2-(2-aminoethylphenyl) bromide to generate dicyclohexylphosphino-2',6 '-di I-propoxy -1,1'-biphenyl dibromide;
2. the reaction of dicyclohexylphosphino-2 ',6'-di I-propoxy -1,1 '-biphenyl dibromide with chloropalladium acid to generate RuPhos Pd G1 palladium ligand;
3. add the generated RuPhos Pd G1 palladium ligand to methyl tert-butyl ether for solvent addition.
Safety Information:
- RuPhos Pd G1 Methyl t-Butyl Ether Adduct is an oxygen-sensitive substance that needs to be protected from light and under an inert atmosphere during operation.
-It has low toxicity, but still needs to be careful to avoid contact with skin, eyes and inhalation.
-Wear appropriate personal protective equipment such as lab gloves, goggles and protective clothing when operating.
-Please store and handle the compound properly and avoid contact with oxygen, flammable substances, strong oxidants, etc.
Nature:
-Appearance: Colorless to light yellow crystal
-Molecular formula: Cover? H? ClNOP? Pd
-Molecular weight: 714.57g/mol
-Melting point: 160-161°C
-Soluble: Soluble in some organic solvents, such as dimethylformamide and dichloromethane
Use:
- RuPhos Pd G1 Methyl t-Butyl Ether Adduct is a commonly used palladium ligand system, which is widely used in organic synthesis reactions, especially negative hydrogenation reactions, hydrogenation coupling reactions and carbonylation reactions.
-The ligand has excellent catalytic activity and selectivity, can catalyze the hydrogenation reaction of a variety of substrates, and help improve the yield of the reaction and the purity of the product.
Preparation Method:
RuPhos Pd G1 Methyl t-Butyl Ether Adduct can be prepared by the following steps:
1. reacting dicyclohexylphosphino-2 ',6'-di I-propoxy -1,1 '-biphenyl with 2-(2-aminoethylphenyl) bromide to generate dicyclohexylphosphino-2',6 '-di I-propoxy -1,1'-biphenyl dibromide;
2. the reaction of dicyclohexylphosphino-2 ',6'-di I-propoxy -1,1 '-biphenyl dibromide with chloropalladium acid to generate RuPhos Pd G1 palladium ligand;
3. add the generated RuPhos Pd G1 palladium ligand to methyl tert-butyl ether for solvent addition.
Safety Information:
- RuPhos Pd G1 Methyl t-Butyl Ether Adduct is an oxygen-sensitive substance that needs to be protected from light and under an inert atmosphere during operation.
-It has low toxicity, but still needs to be careful to avoid contact with skin, eyes and inhalation.
-Wear appropriate personal protective equipment such as lab gloves, goggles and protective clothing when operating.
-Please store and handle the compound properly and avoid contact with oxygen, flammable substances, strong oxidants, etc.
Last Update：2024-04-10 22:29:15
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Product Name: Chloro(2-dicyclohexylphosphino-2',6'-di-i-propoxy-1,1'-biphenyl)[2-(2-aminoethylphenyl)]palladium(II), methyl-t-butylether adduct, min. 98% [RuPhos Pa Request for quotationCAS: 1028206-60-1
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Product Name: Chloro(2-dicyclohexylphosphino-2',6'-di-i-propoxy-1,1'-biphenyl)[2-(2-aminoethylphenyl)]palladium(II), methyl-t-butylether adduct, min. 98% [RuPhos Pa Visit Supplier Webpage Request for quotationCAS: 1028206-60-1
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Product Name: RuPhos Pd G1 Methyl t--Butyl Ether Adduct Visit Supplier Webpage Request for quotation
CAS: 1028206-60-1
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View History
1028206-60-1
1632278-39-7
5-chlorovaIeronitrile
三氟甲基磺酸钪
C.I. Acid Violet 7, disodium salt
1,3-丙二醇
N-Benzyl-Alpha-Phenylethylamine Hydrochloride
新戊酰基乙腈
4,4'-二氯二苯砜
168333-81-1
1632278-39-7
5-chlorovaIeronitrile
三氟甲基磺酸钪
C.I. Acid Violet 7, disodium salt
1,3-丙二醇
N-Benzyl-Alpha-Phenylethylamine Hydrochloride
新戊酰基乙腈
4,4'-二氯二苯砜
168333-81-1