Quinoline, 3-bromo-
3-Bromoquinoline
CAS: 5332-24-1
Molecular Formula: C9H6BrN
Quinoline, 3-bromo- - Names and Identifiers
| Name | 3-Bromoquinoline |
| Synonyms | NSC 3995 AI3-16560 Bromoquinoline 3-BROMOQUINOLINE 3-BROMOQUINLIINE 3-bromo-quinolin 3-Bromoquinoline 3-Bromo-quinoline Quinoline, 3-bromo- (1Z)-1-[(2-chloro-5-methylphenyl)imino]-1H-isoindol-3-amine |
| CAS | 5332-24-1 |
| EINECS | 226-237-1 |
| InChI | InChI=1/C15H12ClN3/c1-9-6-7-12(16)13(8-9)18-15-11-5-3-2-4-10(11)14(17)19-15/h2-8H,1H3,(H2,17,18,19) |
| InChIKey | ZGIKWINFUGEQEO-UHFFFAOYSA-N |
Quinoline, 3-bromo- - Physico-chemical Properties
| Molecular Formula | C9H6BrN |
| Molar Mass | 208.05 |
| Density | 1.533 g/mL at 25 °C (lit.) |
| Melting Point | 13-15 °C (lit.) |
| Boling Point | 274-276 °C (lit.) |
| Flash Point | >230°F |
| Water Solubility | 103mg/L at 25℃ |
| Vapor Presure | 0.196Pa at 25℃ |
| Appearance | Liquid |
| Color | Clear colorless to yellow |
| BRN | 112939 |
| pKa | 2.69(at 25℃) |
| Storage Condition | Keep in dark place,Inert atmosphere,Room temperature |
| Refractive Index | n20/D 1.664(lit.) |
| Use | For pharmaceutical applications |
Quinoline, 3-bromo- - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. S37/39 - Wear suitable gloves and eye/face protection |
| UN IDs | UN2810 |
| WGK Germany | 3 |
| TSCA | Yes |
| HS Code | 29334900 |
Quinoline, 3-bromo- - Reference Information
| LogP | 3.03 |
| NIST chemical information | Information provided by: webbook.nist.gov (external link) |
| EPA chemical information | Information provided by: ofmpub.epa.gov (external link) |
| Bromoquinoline | There are seven positional isomers, and the list of their main physical properties is as follows: ▼ ▲ Name Melting Point (℃) Boiling Point (℃) Soluble 2-bromoquinoline 48~49 Soluble in diethyl ether, chloroform, benzene 3-bromoquinoline 12~15274~276, 95(66.66Pa)4-bromoquinoline 29~30270 (Decomposition) Soluble in dilute acid 5-bromoquinoline 52 (needle crystal) 280 6-bromoquinoline 242787-bromoquinoline 52 (needle crystal) 2908-bromoquinoline 80165~166(2399.79Pa) |
| Use and preparation method | 3-bromoquinoline reacts with mixed acid to generate 3-bromo-5-nitroquinoline, which is oxidized to 5-bromo-2, 3-pyridinedicarboxylic acid when heated with potassium permanganate. 6-bromoquinoline and nitric acid are heated to form 6-bromo-8-nitroquinoline, which is oxidized to 2, 3-pyridinedicarboxylic acid when interacting with potassium permanganate. 2-bromoquinoline is prepared by the reaction of 2-hydroxyquinoline and phosphorus pentabromide. 3-bromoquinoline was prepared by heating quinoline perbromide at 180 ℃. 4-bromoquinoline is prepared by heating 4-hydroxyquinoline with phosphorus pentabromide, or by diazotization reaction of 4-aminoquinoline. 5-bromoquinoline is heated by m-bromoaniline, glycerol, m-bromonitrobenzene and concentrated sulfuric acid, or is produced by 5-aminoquinoline through diazotization reaction. 6-bromoquinoline is prepared by heating p-bromoaniline with glycerol, concentrated sulfuric acid, and p-bromonitrobenzene. 7-bromoquinoline was prepared by diazotization of 7-aminoquinoline. 8-Bromoquinoline is prepared by heating o-bromoaniline, glycerol, concentrated sulfuric acid and o-bromonitrobenzene. Purpose: As an organic synthesis reagent. |
| Use | Used in pharmaceuticals Pharmaceutical and pesticide intermediates |
Last Update：2024-04-09 19:05:09
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View History
Quinoline, 3-bromo-
2H-Azepin-2-one, 7,7'-methylenebis[hexahydro-
1-methyl-1H-pyrazolo[4,3-c]pyridine-4-carboxylic acid
十一烷酸甲酯
医用聚氨酯绷带
2-叔丁基-9,10-二(2-萘基)蒽
3-甲基-3-胺甲基-1-氧杂环丁烷
D-arabino-Hexonic acid, 2,5-anhydro-3,6-dideoxy-, methyl ester (9CI)
2-氨基-2,3-二甲基丁酰胺
5-bromo-4-ethoxy-2-[(4-methoxyphenyl)methoxy]pyridine
2H-Azepin-2-one, 7,7'-methylenebis[hexahydro-
1-methyl-1H-pyrazolo[4,3-c]pyridine-4-carboxylic acid
十一烷酸甲酯
医用聚氨酯绷带
2-叔丁基-9,10-二(2-萘基)蒽
3-甲基-3-胺甲基-1-氧杂环丁烷
D-arabino-Hexonic acid, 2,5-anhydro-3,6-dideoxy-, methyl ester (9CI)
2-氨基-2,3-二甲基丁酰胺
5-bromo-4-ethoxy-2-[(4-methoxyphenyl)methoxy]pyridine