4-氯-3-甲氧基硝基苯
5-Chloro-2-nitroanisole
CAS: 6627-53-8
Molecular Formula: C7H6ClNO3
4-氯-3-甲氧基硝基苯 - Names and Identifiers
| Name | 5-Chloro-2-nitroanisole |
| Synonyms | 5-CHLORO-2-NITROANISOLE 5-Chloro-2-nitroanisole 4-CHLORO-2-METHOXYNITROBENZENE 4-Chloro-3-methoxy-1-nitrobenzene 4-Chloro-2-methoxy-1-nitrobenzene 4-chloro-2-methoxy-1-nitro-benzen 4-chloro-2-methoxy-1-nitro-benzene |
| CAS | 6627-53-8 |
| EINECS | 229-594-1 |
| InChI | InChI=1/C7H6ClNO3/c1-12-7-4-5(8)2-3-6(7)9(10)11/h2-4H,1H3 |
4-氯-3-甲氧基硝基苯 - Physico-chemical Properties
| Molecular Formula | C7H6ClNO3 |
| Molar Mass | 187.58 |
| Density | 1.4219 (rough estimate) |
| Melting Point | 70-72°C(lit.) |
| Boling Point | 289.1±20.0 °C(Predicted) |
| Flash Point | 128.7°C |
| Solubility | Chloroform, Ethyl Acetate |
| Vapor Presure | 0.00389mmHg at 25°C |
| Appearance | Solid |
| Color | Yellow |
| Storage Condition | Sealed in dry,Room Temperature |
| Refractive Index | 1.6000 (estimate) |
| MDL | MFCD00007288 |
| Physical and Chemical Properties | Light yellow crystals. Melting point 82.5 °c. Soluble in hot ethanol, insoluble in cold ethanol. Can be evaporated with water vapor. |
4-氯-3-甲氧基硝基苯 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S37/39 - Wear suitable gloves and eye/face protection S36 - Wear suitable protective clothing. |
| WGK Germany | 3 |
4-氯-3-甲氧基硝基苯 - Reference Information
| EPA chemical substance information | information provided by: ofmpeb.epa.gov (external link) |
| Use | organic synthesis intermediates. |
| production method | 5-nitro-2-aminoanisole was diazotized with sodium nitrite. The diazonium salt solution is added to a warm solution of cuprous chloride (which may be prepared from copper sulfate, sodium chloride, sodium bisulfite, and sodium hydroxide) under vigorous stirring. The reaction was heated again for 1H after the nitrogen evolution was stopped. The reactant was distilled with steam, and the distillate was cooled and crystallized, filtered and dried to obtain 2-chloro-5-nitroanisole in a yield of 80%. |
Last Update：2024-04-09 19:05:13
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View History
4-氯-3-甲氧基硝基苯
LEAD SUBACETATE, REAGENT (ACS)LEAD SUBACETATE, REAGENT (ACS)LEAD SUBACETATE, REAGENT (ACS)LEAD SUBACETATE, REAGENT (ACS)
2-((叔丁氧基羰基)(甲基)氨基)-3-甲基-3-苯基丁酸
4-(5-氯吡啶-2-基氨基甲酰基)苯基硼酸
[(2-METHYLPHENYL)METHYL]-TRIPHENYLPHOSPHONIUM CHLORIDE
((S)-2-((1-(7-甲基-2-吗啉代-4-氧代-4H-吡啶并[1,2-A]嘧啶-9-基)乙基
1-丁基-2-(2-[3-[2-(1-丁基-1H-苯并[CD]吲哚-2-亚基)乙亚基]-2-氯-环己烯-1-基]乙烯基)苯并[CD]吲哚鎓四氟硼酸盐
1-Iodo-2-methoxybenzene, 2-Iodophenyl methyl ether
(吡咯烷-鎓-1-基甲基)三氟硼酸内盐
(2-氟代-5-(吗啉甲基)苯基)硼酸
LEAD SUBACETATE, REAGENT (ACS)LEAD SUBACETATE, REAGENT (ACS)LEAD SUBACETATE, REAGENT (ACS)LEAD SUBACETATE, REAGENT (ACS)
2-((叔丁氧基羰基)(甲基)氨基)-3-甲基-3-苯基丁酸
4-(5-氯吡啶-2-基氨基甲酰基)苯基硼酸
[(2-METHYLPHENYL)METHYL]-TRIPHENYLPHOSPHONIUM CHLORIDE
((S)-2-((1-(7-甲基-2-吗啉代-4-氧代-4H-吡啶并[1,2-A]嘧啶-9-基)乙基
1-丁基-2-(2-[3-[2-(1-丁基-1H-苯并[CD]吲哚-2-亚基)乙亚基]-2-氯-环己烯-1-基]乙烯基)苯并[CD]吲哚鎓四氟硼酸盐
1-Iodo-2-methoxybenzene, 2-Iodophenyl methyl ether
(吡咯烷-鎓-1-基甲基)三氟硼酸内盐
(2-氟代-5-(吗啉甲基)苯基)硼酸