中文名 | 松酯醇二葡萄糖苷 |
英文名 | Pinoresinol diglucoside |
别名 | 松酯醇二葡萄糖苷 松脂醇二葡萄糖苷 松脂醇双吡喃O葡萄糖苷 松脂醇二葡萄糖苷(标准品) 松脂醇二葡萄糖苷, 来源于杜仲 松酯醇二葡萄糖苷,松脂醇二葡萄糖苷 松脂醇二葡萄糖苷,松酯醇二葡萄糖苷 PINORESINOL DIGLUCOSIDE 松脂醇二葡萄糖苷 |
英文别名 | PINONIC ACID(RG) Pinoresinol diglucoside PINORESINOL DIGLUCOPYRANOSIDE(P) PINORESINOL DIGLUCOSIDE(P)(PLEASE CALL) PINORESINOL DIGLUCOPYRANOSIDE(P)(Please Call) β-D-Glucopyranoside, [(1S,3aR,4S,6aR)-tetrahydro-1H,3H-furo[3,4-c]furan-1,4-diyl]bis(2-methoxy-4,1-phenylene) bis- beta-D-Glucopyranoside, (tetrahydro-1H,3H-furo(3,4-c)furan-1,4-diyl)bis(2-methoxy-4,1-phenylene) bis-, (1S-(1alpha,3aalpha,4alpha,6aalpha))- 4-{(1S,3aR,4S,6aR)-4-[4-(beta-D-glucopyranosyloxy)-3-methoxyphenyl]tetrahydro-1H,3H-furo[3,4-c]furan-1-yl}-2-methoxyphenyl beta-D-glucopyranoside (2S,3R,4S,5S,6R)-2-[4-[(3S,3aR,6S,6aR)-6-[3-methoxy-4-[(2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyphenyl]-1,3,3a,4,6,6a-hexahydrofuro[3,4-c]furan-3-yl]-2-methoxyphenoxy]-6-(hydroxymethyl)oxane-3,4,5-triol |
CAS | 63902-38-5 |
化学式 | C32H42O16 |
分子量 | 682.67 |
InChI | InChI=1/C32H42O16/c1-41-19-7-13(3-5-17(19)45-31-27(39)25(37)23(35)21(9-33)47-31)29-15-11-44-30(16(15)12-43-29)14-4-6-18(20(8-14)42-2)46-32-28(40)26(38)24(36)22(10-34)48-32/h3-8,15-16,21-40H,9-12H2,1-2H3/t15-,16-,21+,22+,23+,24+,25-,26-,27+,28+,29+,30+,31+,32+/m0/s1 |
密度 | 1.498 |
熔点 | 250-251 °C |
沸点 | 917.3±65.0 °C(Predicted) |
比旋光度 | -27.3 (c, 0.54 in H2O) |
闪点 | 509℃ |
蒸汽压 | 0mmHg at 25°C |
溶解度 | DMSO (微溶),甲醇 (微溶,加热),水 (微溶) |
折射率 | 1.632 |
酸度系数 | 12.50±0.70(Predicted) |
存储条件 | Hygroscopic, -20°C Freezer, Under inert atmosphere |
稳定性 | 吸湿性 |
外观 | 固体 |
颜色 | Pale Beige to Light Beige |
物化性质 | 白色结晶粉末,易溶于沸水,略溶于冷水,不溶于乙醇、乙醚等有机溶剂,来源于杜仲。 |
MDL号 | MFCD06656077 |
海关编号 | 29389090 |
参考资料 展开查看 | 1. 刘蔚 常杰 武毅君 等. 健骨痛消丸中活性成分的检测及其抗凝血作用的研究[J]. 河南大学学报(医学版) 2020年39卷2期 80-84页 2020. 2. 资文, 刘韶, 彭应枝. 基于指纹图谱和化学计量学技术筛选张家界产杜仲的标志性成分[J]. 中药材, 2015, 38(009):1831-1834. 3. 刘蕊, 刘韶, 彭应枝,等. 斜率校正"一测多评法"同时测定杜仲中京尼平苷酸、绿原酸、京尼平苷和松脂素二葡萄糖苷的含量[J]. 中国医院药学杂志, 2016, v.36(07):8-13. 4. 王媚,边敏琦,邹俊波,崔春利,张小飞,史亚军,郭东艳,乔安平,贾小刚.UPLC-ESI-MS/MS法同时测定强力定眩胶囊中的7个指标成分[J].化学与生物工程,2020,37(12):63-68. 5. 刘锟,王健英,魏莉,潘颖宜,袁颖.HPLC法测定杜仲皮、叶、雄花中8种成分[J].中成药,2021,43(03):686-691. 6. He, Mingzhen, et al. "Application of characteristic ion filtering with ultra-high performance liquid chromatography quadrupole time of flight tandem mass spectrometry for rapid detection and identification of chemical profiling in Eucommia ulmoides Oliv." 7. Chen, Yazhen, et al. "Effect of roasting and in vitro digestion on phenolic profiles and antioxidant activity of water-soluble extracts from sesame." Food and Chemical Toxicology 139 (2020): 111239.https://doi.org/10.1016/j.fct.2020.111239 8. [IF=5.645] Guoqiang Cui et al."Turpentine as an alternative solvent for the extraction of gutta-percha from Eucommia ulmoides barks."Ind Crop Prod. 2018 Oct;121:142 9. [IF=4.759] Mingzhen He et al."Application of characteristic ion filtering with ultra-high performance liquid chromatography quadrupole time of flight tandem mass spectrometry for rapid detection and identification of chemical profiling in Eucommia ulmoides Oliv."J C 10. [IF=6.529] Qi Huang et al."Systematic investigation of the pharmacological mechanism for renal protection by the leaves of Eucommia ulmoides Oliver using UPLC-Q-TOF/MS combined with network pharmacology analysis."Biomed Pharmacother. 2021 Aug;140:111735 11. [IF=6.023] Yazhen Chen et al."Effects of thermal preparation and in vitro digestion on lignan profiles and antioxidant activity in defatted-sesame meal."Food Chem Toxicol. 2019 Jun;128:89 12. [IF=6.023] Yazhen Chen et al."Effect of roasting and in vitro digestion on phenolic profiles and antioxidant activity of water-soluble extracts from sesame."Food Chem Toxicol. 2020 May;139:111239 13. [IF=4.759] Yueping Jiang et al."Application of multifold characteristic ion filtering combined with statistical analysis for comprehensive profiling of chemical constituents in anti-renal interstitial fibrosis I decoction by ultra-high performance liquid chromatogra 14. [IF=3.935] Yi Zhong et al."A strategy for identifying effective and risk compounds of botanical drugs with LC-QTOF-MS and network analysis: A case study of Ginkgo biloba preparation."J Pharmaceut Biomed. 2021 Jan;193:113759 15. [IF=3.205] Jia Jia et al."Screening of anti-complement active ingredients from Eucommia ulmoides Oliv. branches and their metabolism in vivo based on UHPLC-Q-TOF/MS/MS."J Chromatogr B. 2019 Aug;1124:26 16. [IF=3.352] Mi-jun Peng et al."Dietary supplementation Eucommia ulmoides extract at high content served as a feed additive in the hens industry."Poultry Sci. 2021 Dec;:101650 17. [IF=4.451] Xue-song Wang et al."The antihypertensive effects of Eucommia ulmoides leaf water/ethanol extracts are chlorogenic acid dependent."Journal of Functional Foods. 2022 Jul;94:105129 |